Variable Field
Fast Sample Shuttling for experiencing and correlating multiple magnetic fields
This
direction of research was initiated with the DYN-IDP project in collaboration with the UMR 7203 of the Ecole Normale
Superieure (Dr. Fabien
Ferrage), and was funded
by the ANR. A fruitfull collaboration with
Prof. Tai-huang
Huang from Academia Sinica allowed us to acquire and adapt a
ultra-fast mechanical sample-shuttling device on our narrowbore (700
MHz) and widebore (500 MHz) high field NMR
spectrometers.
Pioneering work in the field of
high-resolution relaxometry using sample shuttling has
been performed by A. Redfield. Our recent collaboration
with the ENS has produced a recent result using a
pneumatic sample shuttling from Bruker that can be
found: here and here. The collaboration with Academia Sinica has allowed us to demonstrate that the ultra-fast mechanical shuttling
device can be used on a standard 700 MHz system with a 5 mm
cryoprobe and allow the acquisition of high-resolution
protein relaxometry at standard concentrations.
One research direction is to mount a fast sample
shuttling device on various high-field superconducting
magnets and use it to measure the relaxation properties of
matter in high-sensitivity and high-resolution
conditions. Permanent magnet inserts can be used to generate
secondary homogeneous spots inside or outside of the bore
of the superconducting magnet. This possibility will allow
for correlation experiments between the mutliple centers,
with high sensitivity and resolution. The concept is
summarized on the next figure.